Material Analysis · Structure & Spectroscopy

Positron Annihilation Lifetime Spectroscopy (PALS)

Characterise positron lifetime components, vacancy-type defect or free-volume signatures, and relative defect concentration and depth trends using a scope agreed around your sample and decision.

  • Positron lifetime components
  • Vacancy-type defect or free-volume…
  • Relative defect concentration and depth…
  • Positron annihilation lifetime spectroscopy
Representative Positron Annihilation Lifetime Spectroscopy equipment selected for the TESTDOG service catalogue
Price
from£600
per sample, excl. VAT
Turnaround
10 working days
Preparation and scope dependent
Available platforms
AMETEK PLS-SYSTEM
Typical outputs
Lifetime spectrum or Doppler parametersFitted lifetime componentsComparative defect interpretationProcessed spectra

Why this service

What PALS can help you understand

Positron Annihilation Lifetime Spectroscopy is selected when the project needs defensible information on positron lifetime components, vacancy-type defect or free-volume signatures, or relative defect…

01

Positron lifetime components

positron annihilation lifetime spectroscopy

02

Vacancy-type defect or free-volume signatures

Doppler broadening

03

Relative defect concentration and depth trends

variable-energy depth profiling

Choose the scope

Start from the question, not the tool

The method, preparation route and reporting depth depend on what you need to decide.

Positron annihilation lifetime spectroscopy

positron lifetime components

Best used when
positron lifetime components
Typical result
Lifetime spectrum or Doppler parameters
Preparation note
Confirm the applicable standard, dimensions, loading direction and number of replicates.

Common outputs

A result package matched to the decision you need to make

Fields, conditions, processing and file formats are confirmed before work begins.

StandardLifetime spectrum or Doppler parameters

Lifetime spectrum or Doppler parameters reported with the agreed units, sample reference and measurement conditions.

StandardFitted lifetime components

Fitted lifetime components supplied in a labelled format suitable for direct sample or condition comparison.

OptionalComparative defect interpretation

Comparative defect interpretation provided with the processing basis and quality checks agreed during technical review.

OptionalProcessed spectra

Processed spectra included when selected in the confirmed reporting scope.

Example results

What PALS results can look like

PALS result: The plot shows variable energy positron lifetime measurements. a Markovian positron implantation depth profiles, the mean implantation
PALS spectrum

The plot shows variable energy positron lifetime measurements. a Markovian positron implantation depth profiles, the mean implantation.

David J. Keeble et al. · source · CC BY
PALS result: The plot shows experimental positron lifetime spectra. Also showing the deconvolution fit components
PALS spectrum

The plot shows experimental positron lifetime spectra. Also showing the deconvolution fit components.

David J. Keeble et al. · source · CC BY

Sample requirements

What to provide before work begins

Provide representative, clearly labelled samples and identify the decision, feature or comparison that matters.

Suitable sampleSubmission requirementPlanning note
Test coupon / specimenProvide labelled specimens prepared to the agreed geometry, orientation and surface condition.Confirm the applicable standard, dimensions, loading direction and number of replicates.
Device / assemblyProvide a complete labelled device or assembly with drawings, interfaces and operating limits.Confirm power, connections, operating state, access restrictions and permitted disassembly.
Solid / componentProvide a clean, stable and clearly labelled specimen with the target face or region identified.Confirm dimensions, cutting permission and whether the original geometry must be preserved.

Objective: state the decision, comparison or acceptance criterion the work must support.

Handling and access: declare hazards, instability, confidentiality, file constraints or special logistics before dispatch or transfer.

Questions and answers

Common planning decisions

Short answers to issues that can change preparation, scope, timing or interpretation.

What should I send for Positron Annihilation Lifetime Spectroscopy?

Provide test coupon / specimen, device / assembly, solid / component as applicable. Exact quantity, dimensions and preparation are confirmed during technical review.

Which analysis option should I choose?

Choose the mode around the decision you need to make. For positron lifetime components, start with positron annihilation lifetime spectroscopy; add Doppler broadening when comparison or quantification is required.

How long will the test take?

Typical turnaround is 10 working days after sample acceptance and method confirmation.

What can limit the result?

Defect assignments are model-dependent and often non-unique. Quantification benefits from reference samples or complementary microscopy/diffraction.

Configure the service

Send the information needed to scope PALS correctly

  • Sample form, material, dimensions and quantity
  • Feature or decision the result must address
  • Required comparison, acceptance criterion or reference
  • Preferred output and reporting depth
PALS analysisfrom£600

Typical turnaround: 10 working days

Configure & Book