Material Analysis · Structure & Spectroscopy

Pyridine-Adsorbed FTIR Spectroscopy (Py-IR)

Characterise functional groups and molecular vibrations, chemical identity and relative changes, and Bronsted and Lewis acid-site bands for pyridine-FTIR using a scope agreed around your sample and decision.

  • Functional groups and molecular vibrations
  • Chemical identity and relative changes
  • Bronsted and Lewis acid-site bands for…
  • ATR, transmission, reflectance,…
Representative Pyridine-Adsorbed FTIR Spectroscopy equipment selected for the TESTDOG service catalogue
Price
from£60
per sample, excl. VAT
Turnaround
13 working days
Preparation and scope dependent
Available platforms
Bruker INVENIOThermo Fisher Nicolet iS50Shimadzu IRXrossPerkinElmer Frontier FTIR
Typical outputs
Background-corrected FTIR spectraBand assignments and comparative overlaysOptional mapping, library match, or acid-site analysisProcessed spectra

Why this service

What Py-IR can help you understand

Pyridine-Adsorbed FTIR Spectroscopy is selected when the project needs defensible information on functional groups and molecular vibrations, chemical identity and relative changes, or Bronsted and Lewis…

01

Functional groups and molecular vibrations

ATR, transmission, reflectance, microscopy, or gas cell

02

Chemical identity and relative changes

mapping or in-situ reaction cell

03

Bronsted and Lewis acid-site bands for pyridine-FTIR

pyridine adsorption and temperature-programmed desorption

Choose the scope

Start from the question, not the tool

The method, preparation route and reporting depth depend on what you need to decide.

ATR, transmission, reflectance, microscopy, or gas cell

functional groups and molecular vibrations

Best used when
functional groups and molecular vibrations
Typical result
Background-corrected FTIR spectra
Preparation note
Exact mass and any drying or dispersion step are confirmed after technical review.

Common outputs

A result package matched to the decision you need to make

Fields, conditions, processing and file formats are confirmed before work begins.

StandardBackground-corrected FTIR spectra

Background-corrected FTIR spectra reported with the agreed units, sample reference and measurement conditions.

StandardBand assignments and comparative overlays

Band assignments and comparative overlays supplied in a labelled format suitable for direct sample or condition comparison.

OptionalOptional mapping, library match, or acid-site analysis

Optional mapping, library match, or acid-site analysis provided with the processing basis and quality checks agreed during technical review.

OptionalProcessed spectra

Processed spectra included when selected in the confirmed reporting scope.

Example results

What Py-IR results can look like

Py-IR result: The plot shows py-IR spectra of catalysts treated with different concentrations of citric acid at 200 °C and 450 °C
Py-IR spectrum

The plot shows py-IR spectra of catalysts treated with different concentrations of citric acid at 200 °C and 450 °C.

Lingyi Mao et al. · source · CC BY

Sample requirements

What to provide before work begins

Provide representative, clearly labelled samples and identify the decision, feature or comparison that matters.

Suitable sampleSubmission requirementPlanning note
Powder / particlesProvide a dry, homogeneous and clearly labelled sample in a sealed container.Exact mass and any drying or dispersion step are confirmed after technical review.
Film / coatingProvide the coated substrate or a flat film with the test surface and coating side clearly marked.State the substrate, nominal thickness and whether sectioning or mounting is permitted.
Fibre / textileProvide clean, dry fibres or a representative textile section in protective packaging.State the fibre type, orientation and whether cutting, bundling or mounting is acceptable.
Liquid / solutionProvide a sealed, compatible container labelled with composition, concentration and solvent.Declare volatility, corrosivity, suspended solids and any storage or temperature requirement.

Objective: state the decision, comparison or acceptance criterion the work must support.

Handling and access: declare hazards, instability, confidentiality, file constraints or special logistics before dispatch or transfer.

Questions and answers

Common planning decisions

Short answers to issues that can change preparation, scope, timing or interpretation.

What should I send for Pyridine-Adsorbed FTIR Spectroscopy?

Provide powder / particles, film / coating, fibre / textile, liquid / solution as applicable. Exact quantity, dimensions and preparation are confirmed during technical review.

Which analysis option should I choose?

The final method, preparation and reporting scope are confirmed after the sample and project objective have been reviewed.

How long will the test take?

Typical turnaround is 13 working days after sample acceptance and method confirmation.

What can limit the result?

Overlapping bands and sampling-depth differences can limit specificity. FTIR is usually semi-quantitative without matrix-matched calibration.

Configure the service

Send the information needed to scope Py-IR correctly

  • Sample form, material, dimensions and quantity
  • Feature or decision the result must address
  • Required comparison, acceptance criterion or reference
  • Preferred output and reporting depth
Py-IR analysisfrom£60

Typical turnaround: 13 working days

Configure & Book